Focused-Ion Beam (FIB) Transmission Electron Microscopy (TEM) Sample Preparation

Report Number:
ARL-TR-10031

Publish Date:

December 2, 2024

Distribution:

Approved for public release: distribution is unlimited.


Author(s):

Wendy L. Sarney, B. Chad Hornbuckle, and Asher C. Leff

Abstract:

This report explains the basics of focused-ion beam (FIB) sample preparation, and its advantages for fabricating certain types of materials and device structures for scanning transmission electron microscopy (TEM). The FIB used is the Thermo–Fischer Helios 5 at Aberdeen Proving Ground, Maryland. This report has detailed schematic illustrations, pictures, and instructions of the complex steps needed for making high-quality TEM samples with FIB.

File Size: 6 MB
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